Synchrotron microtomography

Synchrotron microtomography (SR-µCT) is a non-destructive 3D imaging technique that allows the internal structure of materials and components to be visualised with micrometric resolution and higher contrast than laboratory microtomography.

Thanks to the intensity and coherence of synchrotron radiation, SR-µCT reveals details that would otherwise be invisible, with unrivalled speed and reliability.

Assests of synchrotron microtomography

  • Micrometre resolution, even on large samples

  • High contrast, even between weakly absorbing materials

  • Fast acquisition, suitable for dynamic monitoring or large series inspections

  • Wide range of sample sizes

  • Reduction of metal artefacts and beam hardening

  • Multi-scale tomography

Synchrotron microtomography measurements and analyses

  • Detection and quantification of porosity, inclusions and internal cracks
  • 3D mapping of microstructure: grains, fibres, phases
  • Inspection and characterisation of coatings and interfaces
  • In situ monitoring (4D): thermal and mechanical transformations in real time
  • Non-destructive material health analysis
  • 3D reconstruction of cracks
  • Weld inspection
  • CAD comparison

Novitom's expertise in synchrotron microtomography

  • Appropriate sample preparation for efficient use of synchrotron beam time
 
  • Optimised imaging protocols, selected according to your requirements: high resolution, high contrast, dynamic tracking
 
  • Advanced 3D data processing: segmentation, pre-trained AI network, quantitative measurements, interpretation
 
  • Directly usable results: beyond images, we provide conclusions focused on processes, reliability and performance
 
  • Comprehensive support: from defining your needs to the final delivery, with over 20 years of experience at your service

Sample types

    Metals and alloys: solid parts, test tubes, coupons, powders, coatings
 
    Polymers and composites: carbon/carbon, SMC, 3D woven, CMC, polymer-metal
 
    Ceramics and glass: dense or porous samples
 
    Pharmaceuticals and cosmetics: tablets, gels, emulsions
 
    Historical and palaeontological objects: archaeological artefacts, palaeontological remains, works of art
 
    Complex assemblies: medical devices, space devices, automotive parts, aeronautical parts
 
    Biological tissues: bones, teeth, soft tissues, plant samples

Examples of synchrotron microtomography analyses

Revealing the hidden structure of tablets with synchrotron X-rays

Revealing the hidden structure of tablets with synchrotron X-rays

A recent study conducted by Xploraytion, Novitom, Merck, and…

Revealing the hidden structure of tablets with synchrotron X-rays

Revealing the hidden structure of tablets with synchrotron X-rays

A recent study conducted by Xploraytion, Novitom, Merck, and…

Some technical characteristics

Synchrotron sources make it easy to achieve advanced technical specifications for samples ranging in size from 0.5 mm to 2 m!

 

  • High resolution: pixel size from a few hundred nm to a few tens of µm.
  • High throughput: with acquisition times ranging from a few tens of seconds to a few minutes.
  • Varied contrasts: absorption, phase with possible reinforcement depending on the issue
  • Wide energy range: high beam intensity even at 300 keV
  • Real-time tomography possible: sample under thermal and mechanical stress, in a controlled environment, etc.

Complementarity with other techniques

Microtomographie rayons-X in situ 

Microtomographie rayons-X (µCT)

Microscopie électronique à balayage basse tension (SEM-FEG)

Microscopie à force atomique (AFM)

Nanotomographie synchrotron

Fluorescence rayons-X en microfaisceaux (µXRF)

Micro-diffraction à rayons X

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Unique knowledge and expertise in analytical sciences and 2D-3D-4D imaging